Salicylic acid using square-wave voltammetry with pre-concentration by solid phase extraction onto magnetite nanoparticles
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Abstract
A pencil lead electrode coupling with nano-magnetite adsorption as pre-concentration and extraction in order to analyze salicylic acid (SA) was demonstrated in this work. The optimum conditions for nano-magnetite (Fe3O4) preparation by co-precipitation of ferrous/ferric ions were studied. The parameters affecting the shape and size of the nano-magnetite particles such as the types of base, addition rate, temperature, stirring rate and pH were optimized. The morphology was characterized by Fourier transform infrared spectroscopy, energy dispersive X-ray spectroscopy and transmission electron microscopy. The application of nano-magnetite as the solid phase extractor for the square-wave voltammetry (SWV) of SA gave good results.
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